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HRID461161

反应详情

EQUATION

反应方程式

HRID 461161 的结构方程式

REACTANTS

反应物

2
结构：CCNC(=S)NCC
HCID2735009

N,N'-Diethylthiourea

C5H12N2S

结构：CC(C)c1ccc(C(=O)CCl)cc1S(N)(=O)=O
HCID22760666

未命名化合物

PRODUCTS

生成物

1
结构：CCN=C1SCC(O)(c2ccc(C(C)C)c(S(N)(=O)=O)c2)N1CC.Cl
HCID22760671

未命名化合物

PROCEDURE

实验过程

5.5 g of 2-chloro-4'isopropyl-3'-sulfamoylacetophenone and 2.2 g of 1,3-diethylthio urea were reacted and worked up as prescribed in Example 12. Colorless solid body, decomposition beginning at 96° C, γC=N 1610 cm-1.

WORKUP

后处理

  1. customat 96° C