HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 2-Chloro-3'-sulfamoylacetophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 3'-Sulfamoyl-diazoacetophenone | HCID 53705814 | — |
| Solvent | Diglyme | HCID 8150 | — |
| Product | 2-Chloro-3'-sulfamoylacetophenone | HCID 22007172 | — |
Reaction Steps
9.5 g of 3'-sulfamoyl-diazoacetophenone were reacted as prescribed in Example 66b) with 37% HCl in diethylene glycol dimethyl ether and worked up. Colorless crystals, melting point: 118° C (from a small amount of ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04061761 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-1ccf32dd43ee4e64bae49bae7b48c108 |
| Source note | uspto-grants-1977_12 |