Diethyl Ether → HCID 54205136, compound

HRID 461167Notes

Reaction equation

HRID 461167 reaction equation
[Cl:1][C:2]1[CH:10]=[CH:9][C:5]([C:6](Cl)=[O:7])=[CH:4][C:3]=1[S:11](=[O:14])(=[O:13])[NH2:12].[N+:15](=[CH2:17])=[N-:16].[CH2:18](OCC)C>>[Cl:1][C:2]1[CH:10]=[CH:9][C:5]([C:6](=[O:7])[CH:17]=[N+:15]=[N-:16])=[CH:4][C:3]=1[S:11](=[O:14])(=[O:13])[NH:12][CH3:18]

Participants

4

Reactant 3

HCID 3283Diethyl EtherHCID 9550DiazomethaneHCID 30179793-(Aminosulfonyl)-4-chlorobenzoyl chloride

Product 1

HCID 54205136HCID 54205136, compound

Procedure

14 g of 4-chloro-3-sulfamoylbenzoylchloride were reacted as prescribed in Example 66b) with diazomethane in diethyl ether and the crystallized precipitate was filtered. Fair yellow crystals, melting point: 174° C (decomposition).

Workup

  1. filtrationthe crystallized precipitate was filtered

Sources & evidence

ORD record
ord-072a75ba4a8a47388177cc8e9378be09
Source dataset
uspto-grants-1977_12
Patent number
US04061761

Reaction notes

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