HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 54205136, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | 3-(Aminosulfonyl)-4-chlorobenzoyl chloride | HCID 3017979 | — |
| Product | HCID 54205136 | HCID 54205136 | — |
Reaction Steps
14 g of 4-chloro-3-sulfamoylbenzoylchloride were reacted as prescribed in Example 66b) with diazomethane in diethyl ether and the crystallized precipitate was filtered. Fair yellow crystals, melting point: 174° C (decomposition).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04061761 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-072a75ba4a8a47388177cc8e9378be09 |
| Source note | uspto-grants-1977_12 |