HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropyl Ether → HCID 22760488, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropyl Ether | HCID 7914 | — |
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | HCID 22760628 | HCID 22760628 | — |
| Reactant | HCID 73997319 | HCID 73997319 | — |
| Product | HCID 22760488 | HCID 22760488 | — |
Reaction Steps
16 g of 3-tert.-butylsulfamoyl-4-chlorobenzoyl chloride were reacted as prescribed in Example 66b) with a solution of diazomethane in diisopropyl ether, sparingly soluble 3'-tert.-butylsulfamoyl-4'-chlorodiazoacetophenone being separated. The crystals were filtered and converted as prescribed in Example 66b) with concentrated HCl in diethyleneglycol dimethyl ether to yield 3'-tert.-butyl-2,4'-dichloroacetophenone. Colorless crystals, melting point: 159° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04061761 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-0d2269cd0f6649fcb3330d2c7652da51 |
| Source note | uspto-grants-1977_12 |