Diazomethane → HCID 54069293, compound

HRID 461194Notes

Reaction equation

HRID 461194 reaction equation
[Cl:1][C:2]1[CH:10]=[CH:9][C:5]([C:6](Cl)=[O:7])=[CH:4][C:3]=1[S:11](=[O:16])(=[O:15])[N:12]([CH3:14])[CH3:13].[N+:17](=[CH2:19])=[N-:18]>C(OCC)C>[Cl:1][C:2]1[CH:10]=[CH:9][C:5]([C:6](=[O:7])[CH:19]=[N+:17]=[N-:18])=[CH:4][C:3]=1[S:11](=[O:16])(=[O:15])[N:12]([CH3:14])[CH3:13]

Participants

4

Reactant 2

HCID 9550DiazomethaneHCID 22760496HCID 22760496, compound

Product 1

HCID 54069293HCID 54069293, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

14.1 g of 4-chloro-3-dimethylsulfamoylbenzoyl-chloride were reacted as prescribed in Example 66b) with diazomethane in diethyl ether and the crystalline product was filtered off. Melting point: 136° - 137° C (decomposition).

Workup

  1. filtrationthe crystalline product was filtered off

Sources & evidence

ORD record
ord-4625e3fb3fa04ac582d4ea2b6c4ae859
Source dataset
uspto-grants-1977_12
Patent number
US04061761

Reaction notes

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