HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diazomethane → 4'-Chloro-3'-dimethylsulfamoyl-diazoacetophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | HCID 22760496 | HCID 22760496 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 4'-Chloro-3'-dimethylsulfamoyl-diazoacetophenone | HCID 54069293 | — |
Reaction Steps
14.1 g of 4-chloro-3-dimethylsulfamoylbenzoyl-chloride were reacted as prescribed in Example 66b) with diazomethane in diethyl ether and the crystalline product was filtered off. Melting point: 136° - 137° C (decomposition).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04061761 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-4625e3fb3fa04ac582d4ea2b6c4ae859 |
| Source note | uspto-grants-1977_12 |