HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromo-2-chloronitrobenzene → 2-Chloro-5-bromoaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromo-2-chloronitrobenzene | HCID 817974 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-Chloro-5-bromoaniline | HCID 3830731 | — |
Reaction Steps
90 g of 5-bromo-2-chloronitrobenzene were hydrogenated in 500 ml of methanol at room temperature and under normal pressure with Raney-Nickel as catalyst and hydrogen. Colorless crystals, melting point: 47° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04061761 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-5dec04d979244d97a4d35c7d8daaa9e1 |
| Source note | uspto-grants-1977_12 |