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HRID461298

反应详情

EQUATION

反应方程式

HRID 461298 的结构方程式

REACTANTS

反应物

2
结构：O=S1(=O)CCCCO1
HCID15411

1,4-Butane sultone

C4H8O3S

结构：CCn1c(C)nc2cc(C#N)ccc21
HCID722385

1-Ethyl-2-methyl-1H-benzimidazole-5-carbonitrile

C11H11N3

PRODUCTS

生成物

1
结构：CCN1c2ccc(C#N)cc2N(CCCCS(=O)(=O)O)C1C
HCID21393100

未命名化合物

收率 72%

PROCEDURE

实验过程

18.6 g (0.1 mole) of compound V and an equimolar amount of 1,4-butanesultone were heated at 140° C for 4 h, then washed with acetone and dried. Melting point: over 260° C. Yield: 72% (23 g).

WORKUP

后处理

  1. washwashed with acetone
  2. customdried
  3. customover 260° C