1,6-Hexanediol → HCID 88826255, compound

Participants

Reaction Steps

The procedures according to Example 1 were repeated using similar apparatus and under essentially similar conditions allowing for the differences in quantities of materials employed. In this example, for the materials of Example 1, 1 mol fumaric acid, 1 mol of 1,6-hexane diol, 0.1% of hypophosphorous acid and 1 mol of triethylphosphite were employed. The product of the reaction had analytical values for acid value, hydroxyl, free triethylphosphite and phosphorus content comparable to those reported in Example 1.

Provenance & Evidence