1-Bromododecane → HCID 21393915, compound

HRID 461452Notes

Reaction equation

HRID 461452 reaction equation
[CH2:1]([N:13]1[CH:17]=[CH:16][N:15]=[C:14]1[CH3:18])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[CH2:19]([Br:31])[CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH3:30]>C(O)(C)C>[Br-:31].[CH2:1]([N:13]1[CH:17]=[CH:16][N:15]([CH2:30][CH2:29][CH2:28][CH2:27][CH2:26][CH2:25][CH2:24][CH2:23][CH2:22][CH2:21][CH2:20][CH3:19])[CH:14]1[CH3:18])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]

Participants

4

Reactant 2

HCID 89191-BromododecaneHCID 150999061-Dodecyl-2-methyl-1H-imidazole

Product 1

HCID 21393915HCID 21393915, compound

Reagents, catalysts & solvents 1

HCID 3776IsopropanolSolvent

Procedure

0.5 mole of 1-n-dodecyl-2-methylimidazole is dissolved in 250 ml of i-propanol and reacted with 0.6 mole of n-dodecyl bromide. The reaction mixture is heated for 10 hours with reflux. Upon separation of the solvent, the remaining residue is washed with ether, suctioned off, and dried.

Workup

  1. temperatureThe reaction mixture is heated for 10 hours
  2. temperaturewith reflux
  3. customUpon separation of the solvent
  4. washthe remaining residue is washed with ether
  5. customdried

Sources & evidence

ORD record
ord-3abca3c7d3a147b380fa369ea9ea7246
Source dataset
uspto-grants-1977_12
Patent number
US04062965

Reaction notes

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