1-Bromooctane → HCID 131710972, compound

HRID 461460Notes

Reaction equation

HRID 461460 reaction equation
[CH2:1]([N:17]1[CH:21]=[CH:20][N:19]=[C:18]1[CH2:22][CH2:23][CH3:24])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16].[CH2:25]([Br:33])[CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH3:32]>>[Br-:33].[CH2:1]([N:17]1[CH:21]=[CH:20][N:19]([CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH3:32])[CH:18]1[CH2:22][CH2:23][CH3:24])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]

Participants

3

Reactant 2

HCID 81401-BromooctaneHCID 21331299HCID 21331299, compound

Product 1

HCID 131710972HCID 131710972, compound

Procedure

1 mole of 1-n-hexadecyl-2-n-propylimidazole and 1.2 moles of n-octyl bromide are heated together at 150° C for 5 hours. Then the unreacted n-octyl bromide is distilled off and the residue is washed with ether.

Workup

  1. distillationThen the unreacted n-octyl bromide is distilled off
  2. washthe residue is washed with ether

Sources & evidence

ORD record
ord-339c49c895cd4ee5a35af80da0015a7d
Source dataset
uspto-grants-1977_12
Patent number
US04062965

Reaction notes

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