Alpha-Methylstyrene → HCID 53915954, compound

HRID 461472Notes

Reaction equation

HRID 461472 reaction equation
[C:1]1([C:7]([CH3:9])=[CH2:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[S:10](Cl)([Cl:13])(=[O:12])=[O:11]>CN(C)C=O>[C:1]1([C:7]([CH3:9])=[CH:8][S:10]([Cl:13])(=[O:12])=[O:11])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

4

Reactant 2

HCID 7407Alpha-MethylstyreneHCID 24648Sulfuryl chloride

Product 1

HCID 53915954HCID 53915954, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

Following the procedure of Preparation A, 2-phenylpropene is reacted with sulfuryl chloride in N,N-dimethylformamide to give 2-phenylpropene-1-sulfonyl chloride, which is then treated with ammonia to give 2-phenylpropene-1-sulfonamide, m.p. 101°-102.5° C.

Sources & evidence

ORD record
ord-cd52d756333341bea881079cd18d03d3
Source dataset
uspto-grants-1977_12
Patent number
US04062960

Reaction notes

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