O-Xylene → HCID 68121339, compound

HRID 461603Notes

Reaction equation

HRID 461603 reaction equation
[NH2:1][N:2]1[CH:6]=[N:5][N:4]=[CH:3]1.[C:7]1([CH3:14])[C:8]([CH3:13])=[CH:9][CH:10]=[CH:11][CH:12]=1>O>[CH:8](=[C:6]1[N:2]([NH2:1])[CH:3]=[N:4][NH:5]1)[CH2:7][CH2:12][CH2:11][CH2:13][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:7][CH3:14]

Participants

4

Reactant 2

HCID 7237O-XyleneHCID 114324-Amino-1,2,4-triazole

Product 1

HCID 68121339HCID 68121339, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

4-amino-1,2,4-triazole (8.4g.), didecyl aldehyde (18.4g.) and xylene (125 ml.) were heated in a Dean Stack apparatus until the evolution of water ceased. Concentration on the rotary afforded the product as a viscous oil which solidified upon cooling. Yield = 25g. m.p. 40°-3°.

Workup

  1. concentrationConcentration on the

Sources & evidence

ORD record
ord-723aa4f4ecc14f63a909d3dfb091366d
Source dataset
uspto-grants-1977_12
Patent number
US04064059

Reaction notes

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