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HRID461664

反应详情

EQUATION

反应方程式

HRID 461664 的结构方程式

REACTANTS

反应物

2
结构：Nc1cc(Cl)c(Cl)cc1[N+](=O)[O-]
HCID81149

4,5-Dichloro-2-nitroaniline

C6H4Cl2N2O2

结构：O=C1C=Cc2c(ccc3ccccc23)C1=O
HCID3080566

1,2-Phenanthrenequinone

C14H8O2

PRODUCTS

生成物

1
结构：Clc1cc2nc3c4ccccc4c4ccccc4c3nc2cc1Cl
HCID21391726

11,12-Dichlorodibenzo[a,c]phenazine

C20H10Cl2N2

收率 99.9%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

When 0.14 mole each of 3,4-dichloro-6-nitroaniline and phenanthrenequinone were reacted by the method of Example 1, 48.8 g. (99.9 percent yield) of 11,12-dichlorodibenzo[a,c]phenazine, mp = 263°-264° C. (DMF), were obtained.