Methanol → HCID 178512939, compound

Participants

Reaction Steps

L-arginine monofluorophosphate was prepared by combining 34.8 gm. of free-base L-arginine with 20 gm. of monofluorophosphoric acid in about 75 ml. of water. The resulting clear syrup was poured into 750 ml. of a mixture of methanol and ethanol. This was allowed to stand over night and the salt was collected by filtration. The resulting L-arginine monofluorophosphate was then rinsed with methanol and air dried.

Provenance & Evidence