HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 178511811, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Phosphorofluoridic acid | HCID 24267 | — |
| Reactant | HCID 178419078 | HCID 178419078 | — |
| Solvent | Ethanol, mixt. with methanol | HCID 18681192 | — |
| Product | HCID 178511811 | HCID 178511811 | — |
Reaction Steps
L-histidine monofluorophosphate was prepared by combining 31 gm. of free-base L-histidine with 20 gm. of monofluorophosphoric acid in about 75 ml. of water. A clear syrup resulted. The syrup was poured into 750 ml. of a methanol-ethanol mixture. The precipitate (L-histidine monofluorophosphate) was collected and vacuum dried in a desiccator.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04064138 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-17e90312b2714341854be25add764976 |
| Source note | uspto-grants-1977_12 |