Furfurylamine → HCID 21392418, compound
Reaction equation
Br[C:2]1[CH:7]=[C:6]([C:8]([Cl:12])=[C:9]([Cl:11])[Cl:10])[C:5]([S:13]([NH2:16])(=[O:15])=[O:14])=[CH:4][C:3]=1[S:17]([NH2:20])(=[O:19])=[O:18].[CH2:21]([NH2:27])[C:22]1[O:26][CH:25]=[CH:24][CH:23]=1>>[CH2:21]([NH:27][C:2]1[CH:7]=[C:6]([C:8]([Cl:12])=[C:9]([Cl:11])[Cl:10])[C:5]([S:13]([NH2:16])(=[O:15])=[O:14])=[CH:4][C:3]=1[S:17]([NH2:20])(=[O:19])=[O:18])[C:22]1[O:26][CH:25]=[CH:24][CH:23]=1Participants
3
Procedure
4-Bromo-6-trichlorovinyl-1,3-benzenedisulfonamide and furfurylamine are reacted at 70° C. for 10 hours in analogy to above procedure to give 4-furfurylamino-6-(1,2,2-trichlorovinyl)-1,3-benzenedisulfonamide with m.p. 155°-155° C.
Sources & evidence
- ORD record
- ord-e682378b472b40fbaa0d7ca666e99ec2
- Source dataset
- uspto-grants-1977_12
- Patent number
- US04064239
Reaction notes
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