HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 2,7-Bis(5-piperidinovaleryl)fluorene Dihydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 515311 | HCID 515311 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 2,7-Bis(5-piperidinovaleryl)fluorene Dihydrochloride | HCID 21392947 | — |
Reaction Steps
By the procedure of Example 11, 2,7-bis(5-piperidinovaleryl)fluorene was prepared and dissolved in ether then treated with ethereal HCl to give the desired product which was recrystallized twice from methanolethyl acetate. M.P. 268°-270° C, λmaxEtOH 324, Elcm1% 577.8.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04064347 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-c5b870f614a84ce7a8c9c84cd474c698 |
| Source note | uspto-grants-1977_12 |