Hydrochloric Acid → HCID 21392947, compound

HRID 461959Notes

Reaction equation

HRID 461959 reaction equation
[N:1]1([CH2:7][CH2:8][CH2:9][CH2:10][C:11]([C:13]2[CH:25]=[CH:24][C:23]3[C:22]4[C:17](=[CH:18][C:19]([C:26](=[O:37])[CH2:27][CH2:28][CH2:29][CH2:30][N:31]5[CH2:36][CH2:35][CH2:34][CH2:33][CH2:32]5)=[CH:20][CH:21]=4)[CH2:16][C:15]=3[CH:14]=2)=[O:12])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[ClH:38]>CCOCC>[ClH:38].[ClH:38].[N:1]1([CH2:7][CH2:8][CH2:9][CH2:10][C:11]([C:13]2[CH:25]=[CH:24][C:23]3[C:22]4[C:17](=[CH:18][C:19]([C:26](=[O:37])[CH2:27][CH2:28][CH2:29][CH2:30][N:31]5[CH2:36][CH2:35][CH2:34][CH2:33][CH2:32]5)=[CH:20][CH:21]=4)[CH2:16][C:15]=3[CH:14]=2)=[O:12])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 515311HCID 515311, compound

Product 1

HCID 21392947HCID 21392947, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

By the procedure of Example 11, 2,7-bis(5-piperidinovaleryl)fluorene was prepared and dissolved in ether then treated with ethereal HCl to give the desired product which was recrystallized twice from methanolethyl acetate. M.P. 268°-270° C, λmaxEtOH 324, Elcm1% 577.8.

Sources & evidence

ORD record
ord-c5b870f614a84ce7a8c9c84cd474c698
Source dataset
uspto-grants-1977_12
Patent number
US04064347

Reaction notes

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