HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylpiperidine → HCID 515312, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylpiperidine | HCID 69381 | — |
| Reactant | HCID 21392932 | HCID 21392932 | — |
| Product | HCID 515312 | HCID 515312 | — |
Reaction Steps
Following the procedure of Example 7, 20.2g (0.05 mole) of 2,7-bis(5-chlorovaleryl)fluorene, prepared in Example 2, and 39.6g (0.4 mole) of 4-methylpiperidine were reacted to give the desired product which was recrystallized three times from chloroform-acetone. M.P. 143°-144.5° C, λmaxCHCl3 329, E1cm1% 731.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04064347 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-d5df9229e271419d9a7959058ec0a4ed |
| Source note | uspto-grants-1977_12 |