反应详情

To a solution of 62.4 parts of bis-(β-bromoethyl)amine dihybromide in 160 parts of methanol there were added 37 parts of para-phenoxyaniline. The mixture was refluxed for 10 hours. 10.6 parts of Na2CO3 were then added and the reaction mixture was refluxed for a further 10 hours. After cooling, the precipitate was filtered off, washed with 80 parts of methanol and dried.

1. temperatureThe mixture was refluxed for 10 hours
2. temperaturethe reaction mixture was refluxed for a further 10 hours
3. temperatureAfter cooling
4. filtrationthe precipitate was filtered off
5. washwashed with 80 parts of methanol
6. customdried