HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiophosgene → HCID 21390707, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiophosgene | HCID 10040 | — |
| Reactant | HCID 21942426 | HCID 21942426 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 21390707 | HCID 21390707 | 30% |
Reaction Steps
A solution of 5-(4-aminophenyl)-3-(3-pyridyl)-1,2,4-oxadiazole in tetrahydrofuran is reacted with thiophosgene according to Example 14 to give the title compound in 30% yield, m.p. 121°-123°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04065563 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-90150c5e7e9a46eabce81c66f75ddd76 |
| Source note | uspto-grants-1977_12 |