HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12595616, compound → HCID 12595642, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12595616 | HCID 12595616 | — |
| Reactant | HCID 12595618 | HCID 12595618 | — |
| Product | HCID 12595642 | HCID 12595642 | 75% |
Reaction Steps
Following the procedure of Example 16, but sutstituting 4-(m-tolyl)-4-dimethylaminocyclohexanone ethylene ketal hydroiodide for the 4-(o-tolyl)-4-dimethylaminocyclohexanone ethylene ketal hydroiodide there is obtained the 4-(m-tolyl)-4-dimethylaminocyclohexanone hydroiodide salt in 75% yield after recrystallization from methylene chloride:ethyl acetate; m.p. 172°-174.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04065573 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-c9fa378f0a1443798688fd00c09d5b52 |
| Source note | uspto-grants-1977_12 |