HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thioanisole → HCID 178506884, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thioanisole | HCID 7520 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 178506884 | HCID 178506884 | — |
Reaction Steps
To a solution of 1.17 ml. of thioanisole in 20 ml. of dry tetrahydrofuran were added 8.4 ml. of a 1.2M solution of n-butyllithium in n-hexane at -20° C. and the mixture was stirred at the same temperature of 1.5 hours to give a 0.28M solution of phenylthiomethyllithium in tetrahydrofuran.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04065632 |
| Source dataset | uspto-grants-1977_12 |
| ORD ID | ord-a2b84e137900498fa3034aa88ad675d5 |
| Source note | uspto-grants-1977_12 |