HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 20266223, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | 3-(Benzenesulfonyl)-7-methoxy-2-benzofuran-1(3H)-one | HCID 10957672 | — |
| Reactant | 2-Propanol, 2-methyl-, lithium salt (1:1) | HCID 23664764 | — |
| Product | HCID 20266223 | HCID 20266223 | — |
Reaction Steps
To a magnetically stirred solution of lithium t-butoxide (8.8 mmol, prepared from 8.8 mmol of n-BuLi and 9.0 mmol of t-BuOH in 100 mL of THF), cooled to -78° C., was slowly added a slurry of 7-methoxy-3-phenylsulfonyl-1-(3H)-isobenzofuranone (6) (0.91 g, 3 mmol) in THF (20 mL).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04515720 |
| Source dataset | uspto-grants-1985_05 |
| ORD ID | ord-2bc1679eb84c4ab0acc3a12c7420ade9 |
| Source note | uspto-grants-1985_05 |