HCID 4262289, compound → HCID 13457043, compound

HRID 462378Notes

Reaction equation

HRID 462378 reaction equation
[C:1]1(=[O:11])[C:10]2[CH:5]([CH2:6][CH2:7][CH2:8][CH:9]=2)[CH2:4][CH2:3][CH2:2]1.C1(S([CH:21]2[C:29]3C(=CC=CC=3)C(=O)[O:22]2)(=O)=O)C=CC=CC=1.C1(=O)C2C(CC3C(C=2)=CC2C(=CC=CC=2)C3)CCC1>CN(C)C=O>[C:21]([CH:7]1[CH2:8][CH2:9][CH:10]2[CH:5]([CH2:4][CH:3]=[CH:2][C:1]2=[O:11])[CH2:6]1)(=[O:22])[CH3:29]

Participants

5

Reactant 3

HCID 4262289HCID 4262289, compoundHCID 115428101(2H)-Naphthalenone, 3,4,4a,5,6,7-hexahydro-HCID 53687299HCID 53687299, compound2×

Product 1

HCID 13457043HCID 13457043, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

reacting the hexahydronaphthalenone product with phenylsulfonyl isobenzofuranone to create a hexahydronaphthacenone product having the formula ##STR21## and heating the hexahydronaphthacenone product in dimethylforamide under an oxygen atmosphere to produce the compound.

Workup

  1. customto produce the compound

Sources & evidence

ORD record
ord-27e8403e659a4ffe88c8a8c66dea123a
Source dataset
uspto-grants-1985_05
Patent number
US04515720

Reaction notes

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