HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 20397540, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 8-(2-Chloroethanesulfonyl)-1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluorooctane | HCID 20397537 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 20397540 | HCID 20397540 | — |
Reaction Steps
2-(Perfluorohexyl)ethanyl 2-chloroethanyl sulfone (4.75 g, 10.0 mmole) was dissolved in 25 ml of THF at 30°, and triethylamine (1.52 g, 15.0 mmole) in 10 ml of THF was added in one minute. A white precipitate formed, and was filtered (1.37 g). The solvent was stripped carefully, as some foaming occurred.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04517384 |
| Source dataset | uspto-grants-1985_05 |
| ORD ID | ord-c3683595c59f405c8c1c64c3c3bb343a |
| Source note | uspto-grants-1985_05 |