HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 70400290, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Bromine | HCID 24408 | — |
| Reactant | HCID 13235820 | HCID 13235820 | — |
| Reactant | HCID 20281483 | HCID 20281483 | — |
| Product | HCID 70400290 | HCID 70400290 | — |
Reaction Steps
By the cyclisation procedure described for the preparation of 2-(4-chlorophenyl)-2-bromomethyl-5-prop-1-yltetrahydrofuran (see Example 1), 3-ethyl-4-(4-chlorophenyl)pent-4-en-1-ol (1.20 g), bromine (0.86 g), and pyridine (0.43 g) in dichloromethane gave 2-(4-chlorophenyl)-2-bromo-methyl-3-ethyltetrahydrofuran (1.60 g) as a red oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04518415 |
| Source dataset | uspto-grants-1985_05 |
| ORD ID | ord-8305737ea4e24c048483d16239f72c1d |
| Source note | uspto-grants-1985_05 |