Hydrogen Peroxide → 2H-3,1-Benzoxazin-2-one, 1,4-dihydro-6-(4-((4-chlorophenyl)sulfinyl)butoxy)-4,4-dimethyl-

HRID 463116Notes

Reaction equation

HRID 463116 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([S:8][CH2:9][CH2:10][CH2:11][CH2:12][O:13][C:14]2[CH:15]=[CH:16][C:17]3[NH:22][C:21](=[O:23])[O:20][C:19]([CH3:25])([CH3:24])[C:18]=3[CH:26]=2)=[CH:4][CH:3]=1.[OH:27]O>>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([S:8]([CH2:9][CH2:10][CH2:11][CH2:12][O:13][C:14]2[CH:15]=[CH:16][C:17]3[NH:22][C:21](=[O:23])[O:20][C:19]([CH3:24])([CH3:25])[C:18]=3[CH:26]=2)=[O:27])=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 784Hydrogen PeroxideHCID 132605516-[4-(4-chlorophenylmercapto)-butoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one

Product 1

HCID 132605572H-3,1-Benzoxazin-2-one, 1,4-dihydro-6-(4-((4-chlorophenyl)sulfinyl)butoxy)-4,4-dimethyl-

Procedure

Prepared analogously to Example 2 from 6-[4-(4-chlorophenylmercapto)-butoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one and hydrogen peroxide.

Sources & evidence

ORD record
ord-430a2643307d4ae1b0f69ec6559c7e69
Source dataset
uspto-grants-1985_05
Patent number
US04518597

Reaction notes

Loading…