Hydrogen Peroxide → 6-[4-(3,4-Dichloro-phenylsulfinyl)-butoxy]-4H-3,1-benzoxazin-2-one

HRID 463132Notes

Reaction equation

[Cl:1][C:2]1[CH:3]=[C:4]([S:9][CH2:10][CH2:11][CH2:12][CH2:13][O:14][C:15]2[CH:16]=[CH:17][C:18]3[NH:23][C:22](=[O:24])[O:21][CH2:20][C:19]=3[CH:25]=2)[CH:5]=[CH:6][C:7]=1[Cl:8].[OH:26]O>>[Cl:1][C:2]1[CH:3]=[C:4]([S:9]([CH2:10][CH2:11][CH2:12][CH2:13][O:14][C:15]2[CH:16]=[CH:17][C:18]3[NH:23][C:22](=[O:24])[O:21][CH2:20][C:19]=3[CH:25]=2)=[O:26])[CH:5]=[CH:6][C:7]=1[Cl:8]

Participants

Reactant 2

HCID 784Hydrogen Peroxide

HCID 202817946-[4-(3,4-dichlorophenylmercapto)-butoxy]-4H-3,1-benzoxazin-2-one

Product 1

HCID 132605756-[4-(3,4-Dichloro-phenylsulfinyl)-butoxy]-4H-3,1-benzoxazin-2-one

Procedure

Prepared analogously to Example 2 from 6-[4-(3,4-dichlorophenylmercapto)-butoxy]-4H-3,1-benzoxazin-2-one and hydrogen peroxide.

Sources & evidence

ORD record: ord-f108f9a28a294ec286dbb1b150d4b8f3
Source dataset: uspto-grants-1985_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04518597

Reaction notes

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