Hydrogen Peroxide → 6-(4-Methylsulfinyl-butoxy)-4,4-dimethyl-4H-3,1-benzoxazin-2-one

HRID 463135Notes

Reaction equation

[CH3:1][S:2][CH2:3][CH2:4][CH2:5][CH2:6][O:7][C:8]1[CH:9]=[CH:10][C:11]2[NH:16][C:15](=[O:17])[O:14][C:13]([CH3:19])([CH3:18])[C:12]=2[CH:20]=1.[OH:21]O>>[CH3:1][S:2]([CH2:3][CH2:4][CH2:5][CH2:6][O:7][C:8]1[CH:9]=[CH:10][C:11]2[NH:16][C:15](=[O:17])[O:14][C:13]([CH3:18])([CH3:19])[C:12]=2[CH:20]=1)=[O:21]

Participants

Reactant 2

HCID 784Hydrogen Peroxide

HCID 132605326-(4-Methylmercapto-butoxy)-4,4-dimethyl-4H-3,1-benzoxazin-2-one

Product 1

HCID 132605786-(4-Methylsulfinyl-butoxy)-4,4-dimethyl-4H-3,1-benzoxazin-2-one

Procedure

Prepared analogously to Example 2 from 6-(4-methylmercapto-butoxy)-4,4-dimethyl-4H-3,1-benzoxazin-2-one and hydrogen peroxide.

Sources & evidence

ORD record: ord-b65eccd33df54c0e92bb7d69504a2188
Source dataset: uspto-grants-1985_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04518597

Reaction notes

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