Hydrogen Peroxide → 6-[4-(4-Acetamido-phenylsulfinyl)-butoxy]-4,4-dicyclohexyl-4H-3,1-benzoxazin-2-one

HRID 463137Notes

Reaction equation

HRID 463137 reaction equation
[C:1]([NH:4][C:5]1[CH:10]=[CH:9][C:8]([S:11][CH2:12][CH2:13][CH2:14][CH2:15][O:16][C:17]2[CH:18]=[CH:19][C:20]3[NH:25][C:24](=[O:26])[O:23][C:22]([CH:33]4[CH2:38][CH2:37][CH2:36][CH2:35][CH2:34]4)([CH:27]4[CH2:32][CH2:31][CH2:30][CH2:29][CH2:28]4)[C:21]=3[CH:39]=2)=[CH:7][CH:6]=1)(=[O:3])[CH3:2].[OH:40]O>>[C:1]([NH:4][C:5]1[CH:6]=[CH:7][C:8]([S:11]([CH2:12][CH2:13][CH2:14][CH2:15][O:16][C:17]2[CH:18]=[CH:19][C:20]3[NH:25][C:24](=[O:26])[O:23][C:22]([CH:33]4[CH2:38][CH2:37][CH2:36][CH2:35][CH2:34]4)([CH:27]4[CH2:28][CH2:29][CH2:30][CH2:31][CH2:32]4)[C:21]=3[CH:39]=2)=[O:40])=[CH:9][CH:10]=1)(=[O:3])[CH3:2]

Participants

3

Reactant 2

HCID 784Hydrogen PeroxideHCID 132605376-[4-(4-Acetamido-phenylmercapto)-butoxy]-4,4-dicyclohexyl-4H-3,1-benzoxazin-2-one

Product 1

HCID 202817816-[4-(4-Acetamido-phenylsulfinyl)-butoxy]-4,4-dicyclohexyl-4H-3,1-benzoxazin-2-one

Procedure

Prepared analogously to Example 2 from 6-[4-(4-acetamido-phenylmercapto)-butoxy]-4,4-dicyclohexyl-4H-3,1-benzoxazin-2-one and hydrogen peroxide.

Sources & evidence

ORD record
ord-d41b74bd6a674ab88c01fab53fed60df
Source dataset
uspto-grants-1985_05
Patent number
US04518597

Reaction notes

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