Hydrogen Peroxide → 6-[4-(4-Methyl-phenylsulfinyl)-butoxy]-4,4-dicyclohexyl-4H-3,1-benzoxazin-2-one

HRID 463138Notes

Reaction equation

HRID 463138 reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([S:8][CH2:9][CH2:10][CH2:11][CH2:12][O:13][C:14]2[CH:15]=[CH:16][C:17]3[NH:22][C:21](=[O:23])[O:20][C:19]([CH:30]4[CH2:35][CH2:34][CH2:33][CH2:32][CH2:31]4)([CH:24]4[CH2:29][CH2:28][CH2:27][CH2:26][CH2:25]4)[C:18]=3[CH:36]=2)=[CH:4][CH:3]=1.[OH:37]O>>[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([S:8]([CH2:9][CH2:10][CH2:11][CH2:12][O:13][C:14]2[CH:15]=[CH:16][C:17]3[NH:22][C:21](=[O:23])[O:20][C:19]([CH:24]4[CH2:25][CH2:26][CH2:27][CH2:28][CH2:29]4)([CH:30]4[CH2:31][CH2:32][CH2:33][CH2:34][CH2:35]4)[C:18]=3[CH:36]=2)=[O:37])=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 784Hydrogen PeroxideHCID 132605336-[4-(4-methylphenylmercapto)-butoxy]-4,4-dicyclohexyl-4H-3,1-benzoxazin-2-one

Product 1

HCID 132605816-[4-(4-Methyl-phenylsulfinyl)-butoxy]-4,4-dicyclohexyl-4H-3,1-benzoxazin-2-one

Procedure

Prepared analogously to Example 2 from 6-[4-(4-methylphenylmercapto)-butoxy]-4,4-dicyclohexyl-4H-3,1-benzoxazin-2-one and hydrogen peroxide.

Sources & evidence

ORD record
ord-60d18fca99e04d0f9896fd1cc7d668c2
Source dataset
uspto-grants-1985_05
Patent number
US04518597

Reaction notes

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