Hydrogen Peroxide → 6-[4-(3,4-Dichloro-phenylsulfinyl)-butoxy]-4,4-dicyclohexyl-4H-3,1-benzoxazin-2-one

HRID 463140Notes

Reaction equation

HRID 463140 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([S:9][CH2:10][CH2:11][CH2:12][CH2:13][O:14][C:15]2[CH:16]=[CH:17][C:18]3[NH:23][C:22](=[O:24])[O:21][C:20]([CH:31]4[CH2:36][CH2:35][CH2:34][CH2:33][CH2:32]4)([CH:25]4[CH2:30][CH2:29][CH2:28][CH2:27][CH2:26]4)[C:19]=3[CH:37]=2)[CH:5]=[CH:6][C:7]=1[Cl:8].[OH:38]O>>[Cl:1][C:2]1[CH:3]=[C:4]([S:9]([CH2:10][CH2:11][CH2:12][CH2:13][O:14][C:15]2[CH:16]=[CH:17][C:18]3[NH:23][C:22](=[O:24])[O:21][C:20]([CH:25]4[CH2:30][CH2:29][CH2:28][CH2:27][CH2:26]4)([CH:31]4[CH2:32][CH2:33][CH2:34][CH2:35][CH2:36]4)[C:19]=3[CH:37]=2)=[O:38])[CH:5]=[CH:6][C:7]=1[Cl:8]

Participants

3

Reactant 2

HCID 784Hydrogen PeroxideHCID 132605216-[4-(3,4-Dichloro-phenylmercapto)-butoxy]-4,4-dicyclohexyl-4H-3,1-benzoxazin-2-one

Product 1

HCID 132605836-[4-(3,4-Dichloro-phenylsulfinyl)-butoxy]-4,4-dicyclohexyl-4H-3,1-benzoxazin-2-one

Procedure

Prepared analogously to Example 2 from 6-[4-(3,4-dichloro-phenylmercapto)-butoxy]-4,4-dicyclohexyl-4H-3,1-benzoxazin-2-one and hydrogen peroxide.

Sources & evidence

ORD record
ord-04fd87c0c2984f529201e04922b9423b
Source dataset
uspto-grants-1985_05
Patent number
US04518597

Reaction notes

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