Hydrogen Peroxide → 6-[5-(3,4-Dichloro-phenylsulfinyl)-pentoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one

HRID 463146Notes

Reaction equation

[Cl:1][C:2]1[CH:3]=[C:4]([S:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][O:15][C:16]2[CH:17]=[CH:18][C:19]3[NH:24][C:23](=[O:25])[O:22][C:21]([CH3:27])([CH3:26])[C:20]=3[CH:28]=2)[CH:5]=[CH:6][C:7]=1[Cl:8].[OH:29]O>>[Cl:1][C:2]1[CH:3]=[C:4]([S:9]([CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][O:15][C:16]2[CH:17]=[CH:18][C:19]3[NH:24][C:23](=[O:25])[O:22][C:21]([CH3:26])([CH3:27])[C:20]=3[CH:28]=2)=[O:29])[CH:5]=[CH:6][C:7]=1[Cl:8]

Participants

Reactant 2

HCID 784Hydrogen Peroxide

HCID 132605446-[5-(3,4-dichlorophenylmercapto)-pentoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one

Product 1

HCID 132605936-[5-(3,4-Dichloro-phenylsulfinyl)-pentoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one

Procedure

Prepared analogously to Example 2 from 6-[5-(3,4-dichlorophenylmercapto)-pentoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one and hydrogen peroxide.

Sources & evidence

ORD record: ord-f2b1e592e6c04f40ae2a6800d2b2f6bd
Source dataset: uspto-grants-1985_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04518597

Reaction notes

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