Hydrogen Peroxide → 7-[4-(2-Pyridylsulfinyl)-butoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one

HRID 463201Notes

Reaction equation

[N:1]1[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[S:7][CH2:8][CH2:9][CH2:10][CH2:11][O:12][C:13]1[CH:25]=[CH:24][C:16]2[C:17]([CH3:23])([CH3:22])[O:18][C:19](=[O:21])[NH:20][C:15]=2[CH:14]=1.[OH:26]O>>[N:1]1[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[S:7]([CH2:8][CH2:9][CH2:10][CH2:11][O:12][C:13]1[CH:25]=[CH:24][C:16]2[C:17]([CH3:22])([CH3:23])[O:18][C:19](=[O:21])[NH:20][C:15]=2[CH:14]=1)=[O:26]

Participants

Reactant 2

HCID 784Hydrogen Peroxide

HCID 202817217-[4-(2-Pyridylmercapto)-butoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one

Product 1

HCID 202818237-[4-(2-Pyridylsulfinyl)-butoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one

Procedure

Prepared analogously to Example 2 from 7-[4-(2-pyridylmercapto)-butoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one and hydrogen peroxide.

Sources & evidence

ORD record: ord-b76d527142d243ce8ee547d890e590ea
Source dataset: uspto-grants-1985_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04518597

Reaction notes

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