HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → 1-[4-(4-Chlorophenyl)-2-methanesulfonyloxy-n-butyl]imidazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-[4-(4-Chlorophenyl)-2-(methanesulfonyloxy)-n-butyl]imidazole hydrochloride | HCID 20282574 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 1-[4-(4-Chlorophenyl)-2-methanesulfonyloxy-n-butyl]imidazole | HCID 20282243 | — |
Reaction Steps
1-[4-(4-Chlorophenyl)-2-methanesulfonyloxy-n-butyl]imidazole hydrochloride (3.65 g) (prepared in Preparation 10) in methylene chloride (50 ml) was shaken with excess 10% aqueous potassium carbonate solution until no solid remained. The organic layer was separated, dried (MgSO4) and evaporated to give 1-[4-(4-chlorophenyl)-2-methanesulfonyloxy-n-butyl]imidazole as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04518607 |
| Source dataset | uspto-grants-1985_05 |
| ORD ID | ord-30ecff05fe8a4cde836f81e658ca5416 |
| Source note | uspto-grants-1985_05 |