HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 54247622, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | HCID 13457330 | HCID 13457330 | — |
| Reactant | HCID 178418790 | HCID 178418790 | — |
| Product | HCID 54247622 | HCID 54247622 | — |
Reaction Steps
A solution of 1-[4-(4-chlorophenyl)-2-(4-aminophenylthio)-n-butyl]imidazole (680 mg) and 1 ml of ethyl)isothiocyanate in 20 ml of tetrahydrofuran was heated overnight under gentle reflux. The solvent was then evaporated and the residue chromatographed on silica gel eluting with 2.2% water in ethyl acetate to give 1-[4-(4-chlorophenyl)-2-(4-ethylaminothiocarbonylaminophenylthio)-n-butyl]imidazole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04518607 |
| Source dataset | uspto-grants-1985_05 |
| ORD ID | ord-619cc067e7404e9f9bf37db5674b13d5 |
| Source note | uspto-grants-1985_05 |