Phosphorus oxychloride → HCID 593520, compound

HRID 4633Notes

Reaction equation

HRID 4633 reaction equation
[CH2:1]([NH:3][C:4]([NH:6][NH:7][C:8]([NH:10][CH2:11][CH2:12][CH2:13][O:14][C:15]1[CH:20]=[CH:19][CH:18]=[C:17]([CH2:21][N:22]2[CH2:27][CH2:26][CH2:25][CH2:24][CH2:23]2)[CH:16]=1)=[O:9])=O)[CH3:2].P(Cl)(Cl)(Cl)=O>>[CH2:1]([NH:3][C:4]1[O:9][C:8]([NH:10][CH2:11][CH2:12][CH2:13][O:14][C:15]2[CH:20]=[CH:19][CH:18]=[C:17]([CH2:21][N:22]3[CH2:27][CH2:26][CH2:25][CH2:24][CH2:23]3)[CH:16]=2)=[N:7][N:6]=1)[CH3:2]

Participants

3

Reactant 2

HCID 24813Phosphorus oxychlorideHCID 13657348N-ethyl-N'-[3-[3-(1-piperidinylmethyl)phenoxy]propyl]-1,2-hydrazine dicarboxamide

Product 1

HCID 593520HCID 593520, compound

Procedure

The compound is prepared by a method analogous to that of Example 40 from N-ethyl-N'-[3-[3-(1-piperidinylmethyl)phenoxy]propyl]-1,2-hydrazine dicarboxamide and phosphorus oxychloride. The analytical values are summarized in Table III.

Sources & evidence

ORD record
ord-11086ec733244a54a276cc40317b0007
Source dataset
uspto-grants-1988_02
Patent number
US04727081

Reaction notes

Loading…