HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 20283012, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 20283020 | HCID 20283020 | — |
| Catalyst | Iron | HCID 23925 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 20283012 | HCID 20283012 | 118.8% |
Reaction Steps
The thus obtained 2-hexadecylcarbamoyl-4-(2-nitrophenoxy)-1-naphthol (10 g) was reduced with iron in isopropanol. The reaction mixture was filtered, condensed under reduced pressure and added with concentrated hydrochloric acid, and precipitated crystals were collected by a filtration to give 5.8 g of 4-(2-aminophenoxy)-2-hexadecylcarbamoyl-1-naphthol hydroxide. Yield: 57%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04518682 |
| Source dataset | uspto-grants-1985_05 |
| ORD ID | ord-4ecf249b607d43aab845f2f968da32e3 |
| Source note | uspto-grants-1985_05 |