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HRID463331

反应详情

EQUATION

反应方程式

HRID 463331 的结构方程式

REACTANTS

反应物

2
结构：O=C([O-])O.[Na+]
HCID516892

Sodium Bicarbonate

CHNaO3

结构：CCCc1c(OCC(O)COc2ccc3ccc(C(=O)O)cc3c2CCC)ccc(C(C)=O)c1O
HCID20282932

未命名化合物

PRODUCTS

生成物

1
结构：CCCc1c(OCC(O)COc2ccc3ccc(C(=O)[O-])cc3c2CCC)ccc(C(C)=O)c1O.[Na+]
HCID23721273

未命名化合物

收率 85.7%

PROCEDURE

实验过程

7-[3-(4-acetyl-3-hydroxy-2-propylphenoxy)-2-hydroxypropoxy]-8-propylnaphthalene-2-carboxylic acid (9.377 g) was treated with an aqueous solution of sodium bicarbonate (1.640 g) and the resulting solution was freeze-dried to afford sodium 7-[3-(4-acetyl-3-hydroxy-2-propylphenoxy)-2-hydroxypropoxy]-8-propylnaphthalene-2-carboxylate (8.4 g).

WORKUP

后处理

  1. customthe resulting solution was freeze-dried