HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethyl phosphite → HCID 20264366, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethyl phosphite | HCID 31215 | — |
| Reactant | HCID 53773122 | HCID 53773122 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20264366 | HCID 20264366 | — |
Reaction Steps
Following the procedure of Example 2, 5-(4-trifluoromethylphenoxy)benzo-2,1,3-oxadiazole N-oxide (0.7 g) and triethyl phosphite (5 ml) in 75 ml of ethanol are heated under reflux for 2 hours. The reaction is cooled and stripped, and the residue is purified to give 5-(4-trifluoromethylphenoxy)benzo-2,1,3-oxadiazole, m.p. 77°-78°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04544400 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-c9d8dfa175514b8899f081c2b402b831 |
| Source note | uspto-grants-1985_10 |