HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Butanol → HCID 178454804, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Butanol | HCID 263 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 178527059 | HCID 178527059 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 178454804 | HCID 178454804 | 64.8% |
Reaction Steps
A solution of α-hydroxy-β-chloroethylphosphinic acid (2.9 g) and 1-butanol (10.0 g) in benzene (30 ml) was heated for 3 hours with removal of water through a Dean-Stark apparatus. The same work-up as in Example 6 gave 2.60 g (64.8%) of n-butyl α-hydroxy-β-chloroethylphosphinate (Compound No. 82).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04544652 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-bb8bc40edb864365be34705c2d07cf42 |
| Source note | uspto-grants-1985_10 |