Morpholine → HCID 20265051, compound

HRID 463761Notes

Reaction equation

HRID 463761 reaction equation
[NH:1]1[CH2:6][CH2:5][O:4][CH2:3][CH2:2]1.C(N(CC)CC)C.Br[CH2:15][C:16]1[CH:28]=[CH:27][C:19]2[O:20][C:21]([S:23](=[O:26])(=[O:25])[NH2:24])=[CH:22][C:18]=2[CH:17]=1>CO>[N:1]1([CH2:15][C:16]2[CH:28]=[CH:27][C:19]3[O:20][C:21]([S:23](=[O:25])(=[O:26])[NH2:24])=[CH:22][C:18]=3[CH:17]=2)[CH2:6][CH2:5][O:4][CH2:3][CH2:2]1

Participants

5

Reactant 3

HCID 8083MorpholineHCID 8471TriethylamineHCID 20265088HCID 20265088, compound

Product 1

HCID 20265051HCID 20265051, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

A stirred solution of morpholine and triethylamine in methanol is treated with 5-bromomethyl-2-sulfamoylbenzo[b]furan to give the subject compound.

Workup

  1. customto give the subject compound

Sources & evidence

ORD record
ord-e3f62fd8cf0f41d29ceeae32e7761910
Source dataset
uspto-grants-1985_10
Patent number
US04544667

Reaction notes

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