Acetic Acid → HCID 20265068, compound

HRID 463762Notes

Reaction equation

HRID 463762 reaction equation
Br[CH2:2][C:3]1[CH:15]=[CH:14][C:6]2[O:7][C:8]([S:10](=[O:13])(=[O:12])[NH2:11])=[CH:9][C:5]=2[CH:4]=1.[C:16]([O-:19])(=[O:18])[CH3:17].[Na+].C(O)(=O)C>C(N(CC)CC)C>[C:16]([O:19][CH2:2][C:3]1[CH:15]=[CH:14][C:6]2[O:7][C:8]([S:10](=[O:13])(=[O:12])[NH2:11])=[CH:9][C:5]=2[CH:4]=1)(=[O:18])[CH3:17]

Participants

5

Reactant 3

HCID 176Acetic AcidHCID 517045Sodium AcetateHCID 20265088HCID 20265088, compound

Product 1

HCID 20265068HCID 20265068, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

A mixture of 5-bromomethyl-2-sulfamoylbenzo[b]furan, anhydrous sodium acetate and glacial acetic acid (15 ml) is treated with a little triethylamine and the mixture is heated to provide the title compound.

Workup

  1. temperaturethe mixture is heated

Sources & evidence

ORD record
ord-4d4bded478e24c93b8f82a626beb28bb
Source dataset
uspto-grants-1985_10
Patent number
US04544667

Reaction notes

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