HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Chloride → 3-Benzyl-5-methyl-1,3,5-oxadiazinane-2,4,6-trione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | 3-Methyl-1,3,5-oxadiazinane-2,4,6-trione | HCID 20265335 | — |
| Product | 3-Benzyl-5-methyl-1,3,5-oxadiazinane-2,4,6-trione | HCID 20265336 | 83% |
Reaction Steps
The process described in example 1 is carried out. 15.2 g of benzyl chloride (0.12 mole) are added to the obtained solution of the salt of 3-methyl-1,3,5-oxadiazine-2,4,6-trione. After 3 hours of reaction at a temperature of 60° C., one obtains 19.4 g of 3-methyl-5-benzyl-1,3,5oxadiazine-2,4,6-trione (yield: 83%) which is an asymmetrical disubstituted 1,3,5-oxadiazine trione of the formula (III).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04544743 |
| Source dataset | uspto-grants-1985_10 |
| ORD ID | ord-415fca06f98942c99977c240ccdfba28 |
| Source note | uspto-grants-1985_10 |