Zincchloride → HCID 20263416, compound

Participants

Reaction Steps

To a solution of 7.6 grams of zinc chloride in 100 milliliters of deionized water was added at once a solution of 20 grams of the sodium salt of 3-methylpyrazole-1-carbodithioate in 150 milliliters of deionized water with vigorous stirring. The product precipitated immediately as a yellow solid. The product was collected by filtration, dried and recovered in a yield of 14.5 grams (70 percent of theoretical). The product melted at 151°-153° C., with decomposition. Upon analysis, the product was found to have carbon, hydrogen and nitrogen contents of 31.39, 2.60 and 14.62 percent, respectively, as compared with the theoretical contents of 31.62, 2.65 and 14.75 percent, respectively, as calculated for the above-named compound.

Provenance & Evidence