Sodium Iodide → HCID 13472748, compound

HRID 464018Notes

Reaction equation

HRID 464018 reaction equation
[S-:1][C:2]#[N:3].[Na+].Cl[CH2:6][C:7]([I:11])=[C:8]([I:10])[I:9].[I-].[Na+]>CC(C)=O>[I:11][C:7](=[C:8]([I:10])[I:9])[CH2:6][S:1][C:2]#[N:3]

Participants

5

Reactant 3

HCID 5238Sodium IodideHCID 516871Sodium thiocyanateHCID 13089448HCID 13089448, compound

Product 1

HCID 13472748HCID 13472748, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

9.14 g (0.113 mole) of sodium thiocyanate are dissolved in 200 ml of acetone; 51.4 g (0.113 mole) of 3-chloro-1,1,2-triiodo-1-propene are then added. In addition, 0.2 g of sodium iodide are also introduced as the catalyst. The reaction mixture is stirred at room temperature for 12 hours.

Sources & evidence

ORD record
ord-8ed19d8c9cbe426780139c4f9b9b7870
Source dataset
uspto-grants-1985_10
Patent number
US04545994

Reaction notes

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