Methanesulfonic Acid → HCID 86740361, compound
Reaction equation
[C:1]([NH:4][C:5]1[CH:17]=[CH:16][C:8]([C:9](=[O:15])[CH2:10][NH:11][CH:12]([CH3:14])[CH3:13])=[CH:7][CH:6]=1)(=[O:3])[CH3:2].[CH3:18][S:19]([OH:22])(=[O:21])=[O:20]>>[CH3:18][S:19]([OH:22])(=[O:21])=[O:20].[C:1]([NH:4][C:5]1[CH:17]=[CH:16][C:8]([C:9](=[O:15])[CH2:10][NH:11][CH:12]([CH3:13])[CH3:14])=[CH:7][CH:6]=1)(=[O:3])[CH3:2]Participants
3
Procedure
The N-(4-acetylaminophenacyl)isopropylamine obtained according to Preparation I is reacted with methanesulfonic acid to give N-(4-acetylaminophenacyl)isopropylamine methanesulfonate.
Workup
- customaccording to Preparation I
Sources & evidence
- ORD record
- ord-3ddfa823290e46b782c66453142f5fb2
- Source dataset
- uspto-grants-1985_10
- Patent number
- US04545996
Reaction notes
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